Journal of Peking University(Health Sciences) ›› 2018, Vol. 50 ›› Issue (1): 53-57. doi: 10.3969/j.issn.1671-167X.2018.01.009

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Effects of different surface treatments on the zirconia-resin cement bond strength

LIAO Yu1,2, LIU Xiao-qiang1, CHEN Li1, ZHOU Jian-feng1, TAN Jian-guo1△   

  1. (1. Department of Prosthodontics, 2. Department of General Dentistry Ⅱ, Peking University School and Hospital of Stomatology & National Engineering Laboratory for Digital and Material Technology of Stomatology & Beijing Key Laboratory of Digital Stomatology, Beijing 100081, China)
  • Online:2018-02-18 Published:2018-02-18
  • Contact: TAN Jian-guo E-mail: kqtanjg@bjmu.edu.cn

Abstract: Objective:To evaluate the effects of different surface treatments on the shear bond strength between zirconia and resin cement. Methods: Forty zirconia discs were randomly divided into four groups (10 discs in each group) for different surface treatments: control, no surface treatment; sandblast, applied air abrasion with aluminum oxide particles; ultraviolet (UV), the zirconia sample was placed in the UV sterilizer at the bottom of the UV lamp at 10 mm, and irradiated for 48 h; cold plasma, the discs were put in the cold plasma cabinet with the cold plasma generated from the gas of He for 30 s. Specimens of all the groups were surface treated prior to cementation with Panavia F 2.0 cement. The surface morphology and contact angle of water were measured. The shear bond strengths were tested and the fai-lure modes were examined with a stereomicroscope. Results: Surface morphology showed no difference between the UV/cold plasma group and the control group. Sandblasted zirconia displayed an overall he-terogeneous distribution of micropores. The contact angle of the control group was 64.1°±2.0°. After sandblasting, UV irradiation and cold plasma exposure, the values significantly decreased to 48.8°±2.6°, 27.1°±3.6° and 32.0°±3.3°. The values of shear bond strength of the specimens with sandblasted (14.82±2.01) MPa were higher than those with no treatment (9.41±1.07) MPa with statistically significant difference (P<0.05). The values of shear bond strength of the specimens with UV irradiation (10.02±0.64) MPa were higher than those with no treatment (9.41±1.07) MPa, but without statistically significant difference (P>0.05). The values of cold plasma group (18.34±3.05) MPa were significantly higher than those of control group (9.41±1.07) MPa, even more than those with sandblast(14.82±2.01) MPa (P<0.05). X-ray photoelectron spectroscopy (XPS) showed increase in oxygen (O) and decrease in carbon (C) elements after UV and cold plasma treatment. The surface C/O ratio also decreased after UV and cold plasma treatment. Conclusion: Zirconia specimens treated with UV and cold plasma could significantly improve the hydrophilicity. The surface morphology was unaffec-ted by the UV irradiation and cold plasma treatments. The improvements of ziconia shear bond strength were slight in UV group without statistically significant difference. Cold plasma treatment significantly improved the shear bond strength between zirconia and resin cement.

Key words: Zirconia, Resin cement, Ultraviolet, Plasma, Shear bond strength

CLC Number: 

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